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X-Ray fluorescence analysis of iron gall inks

Version 1.0

Wagner, Barbara; Towarek, Aleksandra; Czajka, Anna, 2026, "X-Ray fluorescence analysis of iron gall inks", https://doi.org/10.58132/MHO6H3, Dane Badawcze UW, V1

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Description

Data was acquired using X-Ray fluorescence spectroscopy method, using Bruker ELIO equipment. Measurement of the manuscripts belonging to the collection of the Central Archives of Historical Records in Warsaw took place in their premises.

Measurement parameters were: time: 180s, energy: 50kV, current: 80um. Rhodium plate of high purity was used to separate folios of the manuscripts and provide collection of signal from a single folio.

Data available in the csv file contains the calibrated energy and subsequent counts related to energy ranges. Each column contains data of a single sample with its name in the top row.

The names of measurements correspond to the name of the manuscript and location of measurement and are illustrated in the file 'XRF_lokalizacja_pomiarow'.

Zip file named 'data' contains raw data from the measurement. *spx data format is unique for the Bruker equipment, yet it is a plain text format and can be accessed using a text editor.

The Project No. 2021/41/B/ST4/02860 funded by The National Science Centre, Poland, in the framework of the OPUS 21 program, hosted by the Biological and Chemical Research Center, University of Warsaw, Poland.

Subject
Chemistry
Keyword

iron-gall ink corrosion, X-ray fluorescence

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1 to 3 of 3 Files
XRF_data.tab
Tabular Data - Original format: Comma Separated Values - 3.6 MB - Mar 9, 2026 - 2 Downloads
License: CC0 Creative Commons Zero 1.0
196 Variables, 4000 Observations - UNF:6:sP84bI+xszsmqMlu/22rHg==
XRF results
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data.zip
ZIP Archive - 1.6 MB - Mar 9, 2026 - 3 Downloads
MD5: 78df6618241aa9365602f6ff8fb1ae52
License: CC0 Creative Commons Zero 1.0
Raw data from spectrometer
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XRF_lokalizacja_pomiarow.pdf
Adobe PDF - 814.4 KB - Mar 9, 2026 - 0 Downloads
MD5: 4a756d906f0d3e4323e0fa699fcc2d22
License: CC BY - Creative Commons Attribution 4.0
Location of measurement points in analysed manuscripts
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