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Zglinicki, Karol; Pilaszkiewicz, Michał; Wrzosek, Agnieszka; Szamałek, Krzysztof; Uścinowicz, Szymon; Szefler, Kazimierz; Nowak, Jarosław; Bylina, Paweł, 2025, "Raw XRD data from: Fe-nodules from the southern Baltic Sea. Morphology, mineralogy and geochemistry", https://doi.org/10.58132/OKMYF4, Dane Badawcze UW, V1
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Raw XRD data from research paper "Fe-nodules from the southern Baltic Sea: morphology, mineralogy and geochemistry". These are raw *.xrdml files which may be opened by notepad (in Windows OS) or Profex software (open-source).
For the analysis of the samples, X-ray diffraction in the Bragg-Brentano configuration was employed using an X'Pert PRO MPD diffractometer (PANalytical B.V., Netherlands) equipped with a cobalt anode tube and an iron filter. The samples were dried, crushed, and ground into powder (90% of particles ≤ 80 μm) using an agate mortar and pestle. The powdered samples were pressed into thin pellets using a back-loading method. Diffractograms were recorded over the angular range of 4° to 78° (2θ) using Co Kα radiation, with a voltage of 40 kV and a current of 30 mA, at a measurement step size of 0.026°/min and a step time of 2 seconds. The total analysis duration was 4 hours.
Dane pierwotne z metody dyfrakcji rentgenowskiej z próbek omawianych w artykule: "Fe-nodules from the southern Baltic Sea: morphology, mineralogy and geochemistry". Pliki w formacie *.xrdml, możliwość wglądu za pomocą notatnika w sysytemie Windows lub programu Profex (open-source).
W celu analizy próbek zastosowano dyfrakcję rentgenowską w układzie Bragg-Brentano dyfraktometrze X’Pert PRO MPD (PANalytical B.V., Holandia) wyposażonym w lampę z anodą kobaltową oraz filtr żelazowy. Próbki osuszono, rozkruszono i zmielono na proszek (90% cząstek ≤ 80 μm) przy użyciu moździerza i tłuczka z agatu. Próbki sproszkowane zostały sprasowane w cienkie płytki metodą załadunku od tyłu. Dyfraktogramy rejestrowano w zakresie kątowym od 4 do 78° (2θ) przy użyciu promieniowania Co Kα, napięciu 40 kV i prądzie 30 mA, z krokiem pomiarowym 0,026°/min i czasem pomiaru 2 s/krok. Czas trwania analizy: 4h
XRD, X-ray diffraction
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